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Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline

Al-Douh, Mohammed Hadi and Osman, Hasnah and Abd Hamid, Shafida (2009) Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline. In: International Conference on Instrumentation, Communications, Information Technology, and Biomedical Engineering (ICICI-BME) 2009, 23-25 Nov 2009 , Bandung, Indonesia.

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Abstract

The reaction of o–vanillin 1 with o-phenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline 2. Intermediate 2 is isolated and obtained as single crystals and the structure was determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including APT, COSY, HMQC and HMBC in CDCl3 and will be discussed.

Item Type: Conference or Workshop Item (Full Paper)
Additional Information: 5980/5354 Proceedings ISBN : 978-979-1344-67-8
Uncontrolled Keywords: 1D & 2D NMR , amino benzeneamine , component , intermediate , synthesis , x-ray crystallography
Subjects: Q Science > QD Chemistry
Kulliyyahs/Centres/Divisions/Institutes (Can select more than one option. Press CONTROL button): Kulliyyah of Science > Department of Biotechnology
Depositing User: Mrs. Shafida Abdul Hamid
Date Deposited: 03 Nov 2011 16:10
Last Modified: 23 Dec 2011 15:00
URI: http://irep.iium.edu.my/id/eprint/5354

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