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Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline

Al-Douh, Mohammed Hadi and Osman, Hasnah and Abd Hamid, Shafida (2009) Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline. In: International Conference on Instrumentation, Communications, Information Technology and Biomedical Engineering (ICICI-BME) 2009, 23-25 November 2009, Institut Teknologi Bandung, Indonesia.

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Abstract

The reaction of benzyl o-vanillin 1 with ophenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3- methoxybenzylidene) benzeneamine 2. The intermediate 2 is isolated and obtained as single crystals and their structures were determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including 13C, COSY, HMQC and HMBC in CDCl3 and will be discussed.

Item Type: Conference or Workshop Item (Full Paper)
Additional Information: 5980/5353
Uncontrolled Keywords: component; synthesis; 1D & 2D NMR; x-ray crystallography; amino benzeneamine; intermediate.
Subjects: Q Science > QD Chemistry
Kulliyyahs/Centres/Divisions/Institutes (Can select more than one option. Press CONTROL button): Kulliyyah of Science > Department of Biotechnology
Depositing User: Mrs. Shafida Abdul Hamid
Date Deposited: 21 Oct 2011 14:45
Last Modified: 21 Nov 2011 22:39
URI: http://irep.iium.edu.my/id/eprint/5353

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